A Mixture for Winter

I wanted to make a new fragrance by blending essential oils.  I realised that I’ve posted several “recipes” for fragrances, but I haven’t said much about how I select and blend the ingredients.  What follows is a description of how I made a fragrance called Winter.  It blends essential oils with some science, some experience, some guesswork, some inspiration, some process, and just a hint of magic.

The First Step

“A journey of a thousand miles begins with a single step”

Lao Tzu (Sixth Century Before Christian Era)

There has to be a first step, something that prompts a creative process.  It could be a theme, a memory, a mood.  You might want to re-create something that you’ve encountered.  Smells are strongly connected with memories, so you may want to create something that invokes a memory.

There may be an ingredient that you want to use.  I’ve picked ingredients at random as the starting point for fragrance blends.  On other occasions I’ve picked an ingredient because it connects with a theme I’ve chosen.  I might pick an ingredient for it’s therapeutic properties.  Most often, I’ll start with an ingredient just because I like the way it smells.

Over the course of a couple of years I worked up blends of essential oils, and sometimes other ingredients, to reflect the changing seasons.  I created eight blends and named them for the eight pagan festivals.  During the second pass through the year I created an alternate blend for Litha.  I did that because someone convinced me that Litha “Is all about the Roses”.  That left me without a name for my first Litha blend, so I called it “Summer”.  My slightly obsessive-compulsive mind was disturbed by the idea of Summer without the other three seasons, so I’ve committed myself to creating blends for Autumn, Winter and Spring.

(Those who know me are sniggering now at the idea that my mind is only slightly obsessive-compulsive.)

Inspiration

I had a theme for my new blend.  It would be Winter.

I had taken the Winter celebrations as my inspiration for a fragrance I called Yule.  That combined the traditions of “bringing in the green” with the spices used in festive fare.  I wanted to make Winter a celebration of other aspects of the season.

The Winters where I live are cold and dark and damp.  (The photo at the top of this post was taken in Alaska.)  It’s very rare that we get snow that reflects the natural light, but we do get frosts.  Sometimes standing water freezes over.  It’s a time to wrap up and go out and walk.  You can see further through the trees when the leaves have fallen.  Returning home to make things in a warm kitchen, or to curl up with a good book, adds to the joy of venturing out.

The bitter Seville oranges that are used to make marmalade start to become available in November.  They can normally still be bought in early February.  Making marmalade is one of the delights of Winter.  It calls for two sessions of activity, each about an hour long, with a couple of hours between while the prepared fruit simmers.  It’s a great social activity, because the two hours in the middle can become a long lunch while the house is filled with scent of oranges.

I had my first ingredient for Winter – Orange.

Guesswork

I already had a second ingredient because I wanted to use Wintergreen.

I didn’t want to create a fragrance in which Wintergreen dominates.  It’s a very assertive smell.  Wintergreen is the dominant smell in the Surgical Spirit sold in the US, and in many liniments and muscle rubs.  It’s medicinal, sharp and penetrating.  Any concoction that majored on Wintergreen would smell like the start of the London Marathon.  However, I had a suspicion that Wintergreen could be a dosing ingredient.

There are some perfume ingredients that smell vile if you encounter them in isolation.  Often they include indole, which is a chemical commonly associated with fecal matter.  Civet is one such ingredient. Ambergris is another. Their value in perfumery is that they work a kind of magic when very tiny amounts are added to a blend of other fragrances. These ingredients are sometimes called fixatives. The process of adding one of these ingredients is called dosing.

Process

Now that I had selected two ingredients, I needed to determine the proportions in which to use them.  There are a couple of ways to work this out.

The first way is to use perfume test strips.  These are strips of absorbent paper that are typically around 150mm long and slightly less than 10mm wide.  The process starts with writing the name of a different ingredient on each of two test strips.  It’s a good idea to add the time of day as well as the ingredient name.  Then add a single drop of each ingredient to its named tester strip.  If you bend the scented end of the test strip upwards slightly, you can put the strip down without the scented end touching anything.

Hold the test strips so the fragranced ends are close together, but fanned out slightly so they don’t touch.  Wave the test strips around for a moment, then bring them close to your nose and smell them.

If one of the ingredients overpowers the other, make up another strip with the ingredient you want to increase.  Add that to the fan of test strips, and smell them again.  Adjust the number of strips of each ingredient until you are happy with the balance.

There is a time dimension to perfumes.  If you leave the scented test strips for a while and then return to them, you may find the balance has changed.  Then you have to decide whether you want your blend to be balanced at the first encounter, or to mature into a balance later.

Another process

I like using test strips for sampling perfumes, but I don’t use them for working out the proportions of ingredients when I’m blending essential oils.  It can be difficult to put consistent quantities on test strips, and (in my opinion) they don’t always represent the way ingredients will interact.  My favoured approach is to mix up small samples of ingredients in different proportions.

I started mixing samples in test-tubes.  It resonated with studying in chemistry laboratories, and with the mad scientist ethos.  Test-tubes have their own challenges.  You can’t put them down unless you put them in a rack or put a stopper in them. Glass test-tubes are expensive. Laboratory grade plastic test tubes don’t react well with neat essential oils. If you have any doubts about whether you should ingest undiluted essential oils or apply them to your skin, take a look at what they did to a plastic test tube:

I use glass vials now. They are relatively inexpensive, and as stable as essential oil bottles.

As the starting point for working out proportions, I label 5 vials with the proportions I’ll put in them. Using Orange and Wintergreen as an example, I mix up the oils as follows:

1 drop Wintergreen, 5 drops Orange
2 drops Wintergreen, 4 drops Orange
3 drops Wintergreen, 3 drops Orange
4 drops Wintergreen, 2 drops Orange
5 drops Wintergreen, 1 drop Orange.

You can smell each of the mixtures to see which you think is balanced.  It sometimes helps to add a little perfumer’s alcohol to each vial, screw down the cap and shake the vial to mix the oils and alcohol.  Dipping the end of a test strip into a vial is a good way to sample the mixtures.  It’s best to wave the test strip around for a moment to reduce the alcohol fumes before you smell it.

It’s quite possible that one ingredient still overpowers the other in a 1-to-5 mixture.  In that case you might want to mix up some more samples with proportions of, say, 1 to 10, 1 to 15 and 1 to 20.

I was reasonably content with a mixture of 1 Wintergreen to 12 Orange at this stage.

Experience and more Guesswork

In Patrick Süskind’s novel Perfume, his character Jean-Baptiste Grenouille blends 12 ingredients as the basis of his perfume. Then he doses the mixture with a thirteenth ingredient. Although the total number of ingredients is not a hard and fast rule, professional perfumers will typically blend about a dozen ingredients.  I’m not a professional.  My blends typically contain 5 – 8 ingredients.

I could systematically work out the proportions of 2 ingredients, then having fixed the proportions the first two I could repeat the process to determine the amount of a third ingredients to add to them.  Then I could fix the proportions of the three ingredients and work out how much of a fourth to add.

Life is too short.  I’m sure some apprentice perfumers go through the extended process to work out a blend.  I’m equally sure that most perfumers, professional or amateur, cut some corners based on experience and guesswork, and then make some final adjustments to their blend.

THE PLAN COMES TOGETHER

I liked the combination of Orange with a small quantity of Wintergreen. But both Orange and Wintergreen are Head notes. They are volatile, fading rapidly. A more balanced blend needs some ingredients that are more persistent, that will linger when the Head notes fade and disappear.

Monkey Business Images/Shutterstock

Returning to my chosen theme of Winter, I wanted my blend to be comforting.  I wanted it to bring to mind dark evenings curled up somewhere warm with hands wrapped around a mug containing a favourite hot drink.  There is an essential oil of Coffee, which is a Heart note and smells much as you would expect concentrated coffee to smell.  To add a Base note that would contribute sweetness to the blend, I chose Oakmoss Resin.

My Winter fragrance was coming together. After mixing up a few test samples, the blend comprised:

12 Orange
1 Wintergreen
4 Coffee
6 Oakmoss.

There’s still something missing. It’s time to take a SWAG (Scientific Wild-Arsed Guess) and try something completely random. I add a drop of Camphor …

Camphor is another of those very difficult ingredients, a little like Wintergreen. It’s rarely used in perfumery, like Wintergreen. It just might work …

With the addition of Camphor, I’m almost content with my blend. I eventually conclude that the Wintergreen is just a little too dominant.  I cut the proportion by half (and because there’s only one drop in the original blend, that means doubling the quantity of all the other ingredients).

Wrapping up

Now I can write up the final recipe and rinse out my trial mixture vials into my latest bottle of Frogs Breath.

I can’t use my blend as a perfume until I have diluted the essential oils with a carrier.  In this case I plan to use perfumer’s alcohol and make a perfume at Eau de Cologne strength (1-5% essential oils in perfumer’s alcohol).  I can make an Eau de Cologne at just under 5% by using one measure of the blend and topping up to 50ml with alcohol.  The mixture needs to be left for a few days to macerate.

The final test is to wear the blend, and try to persuade a few other volunteers to wear it too. Perfume works slightly differently (sometimes very differently) with each individual’s skin chemistry.

Perfume doesn’t have to be worn on a body.  It can be sprayed onto fabric or used as a room spray too.  I’ve recently discovered these refillable sprays.  I keep one with my mask to freshen it up between wearings.  Isn’t that a very 2020 thing to do?

Ostara Handcreme #14

“In Spring the young man’s fancy turns to what women have been thinking about all Winter.”
with apologies to Alfred, Lord Tennyson

We see the first glimpses of Spring at the start of February (in my part of the United Kingdom).  By the time the Spring (Or Vernal) Equinox arrives , Spring has definitely sprung.  This year, the Spring Equinox will fall in the early hours of Friday 20 March.  The days lengthen more rapidly at the Spring Equinox than at any other time of the year.  From the Spring Equinox until the Autumn Equinox we will have more hours of daylight than darkness.

This is ostensibly a post about a hand cream for the Spring Equinox.  The hand cream recipe is the same as the recipe for #14 Handcream and the blend of oils used to fragrance this version is Ostara.   So having fulfilled the promise of this post’s title, let’s follow the Easter Bunny down her rabbit-hole and decorate some eggs.

Down the rabbit hole

The last time I decorated eggs by dying them with onion skins was in Edinburgh in 1980.  I thought I’d better test out what I remembered of the process before posting anything about it, so last weekend I bought half a dozen eggs with light coloured shells, and gathered together some onion skins, some newspaper, some string, and some flower petals.  My collection of flowers included crocus, forsythia, primrose, periwinkle, hornbeam and celandine.

The idea is to stick the petals to the surface of an egg, then wrap the decorated egg with onion skin.

The onion skin-wrapped egg is then wrapped in newspaper to hold the petals and the onion skin in place, and tied into a bundle with string.  The bundles are put in a pan, brought to the boil, and boiled for just a little longer than it would normally take for hard-boiled eggs (maybe 5 minutes).  It can be helpful to weight down the bundles so they don’t float in the pan.

And that’s it.  When the wrapped eggs have cooled down enough to handle, you can unwrap the dyed eggs.  The overall effect is marbled, with the onion skin dye masked where the flower petals have been.

It’s still a little too early for me to find flowers in the garden that will colour the eggs rather than just mask the onion skin dye.  Colours rarely come true with this type of dyeing, but I do remember some of the coloured primulas add shades of red and pink to the overall effect.

Forty years ago:

I managed to find the photos I took the first time I dyed eggs in this way.  Here they are, from prints on Kadachrome paper and collected in an album:

 

Imbolc Handcreme #14

Snowdrops
Snowdrops

This is my goto recipe for a handcreme (“Handcreme #14”).  I produce it with different blends of essential oils to reflect the seasons.  This version celebrates the land waking up at the end of Winter.  I’ve called it Imbolc.

Imbolc falls around the 1st of February in the Northern Hemisphere.  It celebrates the first stirrings of Spring as the days become perceptably longer.

Although I normally describe this as a handcreme, its use isn’t limited to hands.  It’s a classic cold cream that is suitable for hands, face or any other skin that may be prone to dryness.   Rosemary Gladstar gives the proportions of ingredients in a cold cream in her book Herbal Healing for Women.  She called her version her Famous Face Cream:

“The basic proportions of this cream recipe should be about one part group 1 (oil phase) to one part group 2 (water phase).

“In group 1, the oil proportions should be approximately 2 parts liquid oils (such as grapeseed, almond, apricot) to 1 part solid oil (cocoa butter, beeswax, lanolin).”

My Heavy Duty Handcreme #21 is another example of a cold cream.

The ingredients, equipment and method I use to make Handcreme #14 are:

Oil Phase
  • 150ml  Sweet Almond Oil
  • 75ml  Coconut Oil
  • 30g  Beeswax
  • 20g  Shea Butter
  • 7.5ml  Lanolin
Water Phase
  • 150ml  Distilled Witch Hazel
  • 75ml  Aloe Vera Gel
Cool Down
  • 7.5m  Vitamin E oil
  • 20-30 drops of essential oils (see later in this post for the Imbolc blend).
Equipment
  • Two heaproof glass containers, one with a capacity of al least 500ml and the second with a capacity of at least 250ml.  (I use Pyrex jugs.  Mason Jars are also suitable.)
  • An electric oven capable of being set to a temperature of 60-70C, or a shallow pan wide enough to accept the glass containers and a kitchen stove electric hob or gas ring
  • A hand blender or whisk
  • Clean jars for the handcreme
  • Spatula(s)
  • Cloths or paper towels for cleanup.
Method
  1. Measure out your oil phase ingredients into the largest of your two glass containers, and measure out the water phase ingredients into the other glass container.  Put a stirrer into the container with the oils – a spatula or spoon.
  2. Heat the ingredients until all the solid oils and waxes melt.  Either;
    • Put the containers into an electric oven set to about 70C, or;
    • Put the containers in a shallow pan and surround them with water.  Bring the water to the boil on a stove top and reduce the heat so the water simmers gently.
  3. Prepare your containers.
  4. When the solid oils and waxes have melted, take the containers out of the oven or off the stove.  Stir the oils (remembering that the stirrer will be quite hot).
  5. Put your blender or whisk into a pot of hot water to preheat it.
  6. When you start to see the oils solidifying, put your blender or whisk in the container with them.  Whisk or blend as you add the water phase ingredients, keeping use of the whisk or blender to a minimum.
  7. Briefly whisk or blend as the mixture cools.  When it gets to around 40C (when the container will still be warm to touch but not too hot to hold comfortably) add the cool-down ingredients and whisk or blend briefly for the final time.
  8. Pour and scrape your cream into your containers.
  9. Label the containers and keep them in a refrigerator until you want to use your handcreme.
  10. Clean up with hot, soapy water.
Handcreme in containers, labelled and with information slips
Imbolc Handcreme #14

I’ve used Handcreme #14 as the basis of a number of seasonal cosmetics.  In December I added my Yule blend of oils.

For the Imbolc version I started with an Imbolc blend proposed by Amy Blackthorn.  (The blend is published in Amy’s book Blackthorn’s Botanical Magic.)  Amy’s blend has  a base/heart note of Angelica Root, with  heart notes of Basil and head notes of Laurel.  I modified Amy’s blend by adding Tobacco Absolute, Violet Leaf Absolute and a goodly dose of Fir Needle.  I aimed to develop a fragrance with green notes throughout.  I’m quite happy with the results – I developed this blend in 2019 and re-used it this year without modification.

Head notes
  • 16 drops Fir Needle Essential Oil
  • 8 drops Laurel Essential Oil
Heart notes
  • 8 drops Violet Leaf Absolute
  • 8 drops Basil Essential Oil
Bass notes
  • 8 drops Angelica Root Essential Oil
  • 4 drops Tobacco Absolute

To end on a cautionary note – neat essential oils can be highly corrosive.  With very few exceptions they should never be applied to skin unless diluted.  I first made this blend last year in a laboratory grade plastic test tube,  intending to add it to handcreme a few days later.  When I came to use it, the interior of the tube was etched and the base was crazed and cracked.  I mixed up some more in a glass container for my batch of handcreme!

Plastic test tube etched and cracked by essential oils
Cautionary tale of effects of essential oils on plastic

Re-imagining the Winter Solstice

My first venture into making cosmetics was around this time of year.  I spent a couple of days at a workshop offered by Rowan McOnegal.  We made a classic Cold Cream and I added what I considered seasonal essential oils to provide fragance and act as preservatives.  I called it “Yule” because it’s a short word to put on a label.  And it’s what I was trying to evoke with the aromatic oils.

Since my first attempts, my cosmetic recipes have mostly been in two parts:

  • A base of oils, often combined with with water based ingredients
  • Esssential oils to provide fragrance and prevent mould and bacterial growth.

This post briefly explores how a perfume of essential oils is constructed, ending up with a recipe for a blend intended to invoke the the spirit of Yule.

The composition of a perfume

The word “composition” is somehow appropriate for perfume.  The analogy of making music is carried into the words used to describe the process.

Essential oils used in composing perfume are divided into three categories:

  • Head (or Top) notes
  • Heart (or Middle) notes
  • Base (or Bottom) notes.

Head notes are the more volatile oils.  They are the first to catch your attention.  Their impact is immediate, but short-lived.  They are the first to fade, often within minutes.

Heart notes have more staying power than head notes.  They may linger for an hour or two.

Base notes are the least volatile, and may last a day or more.

The categorisation of oils as Head, Heart or Base is not an exact science.  Most fall clearly into one category or another, but some inevitably fall on the cusp between.

There are no hard and fast rules, but a balanced perfume normally contains Head, Heart and Base oils.

Chords

Continuing the musical analogy, a blend of notes of the same category is known as a chord.  So a perfume normally comprises:

  • A chord of Head notes
  • A chord of Heart notes
  • A chord of Base notes.

Perfumeurs often blend individual chords, and then blend the completed chords into the final perfume.  I recognize that I’m an amateur, so  I do not attempt to shortcut this process.

Patrick Süskind presents a slightly stylized version of composition in his novel Perfume.  His ideal perfume comprised 12 individual elements in 4 chords, plus a  final 13th element to complete the perfume.  Perfumeurs would recognise the addition of the 13th ingredient as dosing the blended perfume.

Dosing

In addition to the chords that are blended to produce a perfume, some perfumeurs add very small quantities of particularly assertive ingredients.  Musk, civet and ambrette have been used for dosing.  Musk is virtually unobtainable now, and along with civet raises some significant ethical issues.

Re-imagining Yule
The essence of Ule
The essence of Yule

My 2017 and 2018 Yule blends comprised:

  • A Head note of Nutmeg
  • Heart notes of Clove and Cinnamon
  • A Base note of Frankinsense.

While this produced a suitably festive perfume, I wanted to evoke a couple of the memories of distant Winter celebrations:

  • Oranges were one of my childhood associations with the Winter holidays.  Fresh oranges were not so common (it was a while ago) and mandarin oranges (satsumas) were a seasonal treat.
  • Evergreens connect the Christmas Tree tradition with the older “bringing in the green”.

As well as selecting Bitter Orange and Scotch Piner Needle to go with the oils used in earlier years, I added Corriander.  I wanted to include the seasonal references, but that doesn’t always result in a harmonious blend.  I suspected that a little Corriander would help the other ingredients rub along together.  Bitter Orange, Scotch Pine Needle and Corriander are all Head notes, so while my Heart and Base cords remained the same  my Head note chord now comprised:

  • Bitter Orange
  • Scotch Pine Needle
  • Nutmeg
  • Corriander.

I’ll discuss the process of selecting the proportions of the oils in a perfume in a future post.  In the meantime, here’s the my recipe for (this year’s ) Yule fragrance :

  • 6 Drops Bitter Orange Essential Oil
  • 2 Drops Scotch Pine Needle Essential Oil
  • 3 Drops Nutmeg Essential Oil
  • 4 Drops Coriander Essential Oil
  • 3 Drops Clove Essential Oil
  • 2 Drops Cinnamon Essential Oil
  • 9 Drops Frankinsence Essential Oil